Distillation Labware
Glassware and replacement parts designed to carry out distillations in laboratory settings; includes condensers, distillation heads, receivers, etc. Products are available for various scales and for specialty distillations.
Distillation is a process used widely in the laboratory or in wider working environments for separating or purifying liquids or liquid mixtures based on the different boiling points of individual components.
Distillation Applications:
• Separation and purification of miscible liquid mixtures in organic chemistry
• Drying of solid residues and/or solvent removal
• Fractional distillation of liquids from polymers and petroleum products
• Removal of particulates or other solid contaminants
• As part of a water purification system for production of distilled water for laboratory use
• Specialist steam distillation-based applications such as Kjeldahl analysis of nitrogen and proteins in food, beverage, or environmental samples
What Types of Distillation Equipment Are Available?
Conventional distillation apparatus, typically comprising individual, jointed borosilicate glassware components assembled by the user (depending upon the application), using appropriate clamps, stands, and supports. Most conventional distillation assemblies combine a round-bottomed distilling flask to contain and heat the liquid(s) that require purification, fitted with a stoppered or jointed neck to which is attached a downward-sloping, inclined side-arm for connection to a condensing unit to cool the heated vapors back down to their liquid state. Heating mantles are the preferred heat source for improved temperature control. These conventional distillation units are also available supplied complete and ready-assembled for added convenience and ease of use.
Specialized automated distillation equipment, notably units designed for the determination of volatile acidity and alcoholic strength by volume in wines, musts, and alcoholic beverages, and units designed for Kjeldahl nitrogen or protein determinations.
Chemglass Life Sciences Vacuum Trap, Complete, Trap Bottle 45mm OD x 250mm Overall Length, 16mm OD Side and Inner Tubes, 40/50 Jt.
Vacuum Trap, Complete, Trap Bottle 45mm OD x 250mm Overall Length, 16mm OD Side and Inner Tubes, 40/50 Jt. Two piece vacuum trap connected with an inner and outer joint to facilitate cleaning.
Chemglass Life Sciences Vacuum Trap, Complete, 54mm Body OD x 275mm Overall Length, 25mm OD Side and Inner Tubes, 50/50 Jt.
Vacuum Trap, Complete, 54mm Body OD x 275mm Overall Length, 25mm OD Side and Inner Tubes, 50/50 Jt. Similar to CG-4514, but with the top inlet tube bent at a 90º angle.
Ace Glass, Inc. Head, micro distilling, 20-400 top, 10/10 bottom
Head, micro distilling, 20-400 top, 10/10 bottom
Chemglass Life Sciences Saddles, Berl, 200cc, Porcelain, Distilling Column, Approx. 250 Pieces/Package
Saddles, Berl, 200cc, Porcelain, Distilling Column, Approx. 250 Pieces/Package. Porcelain berl saddles having an O.D. of 8mm. Ideal for vacuum distillation, absorption and extraction. Saddles provide a highly useable surface area, lower gas flow resistance and excellent internal distribution. Available in packages of 200cc and 1000cc boxes.
Chemglass Life Sciences 150mL HW Pressure Vessel, Round Bottom, #15 Internal Thread, Vessel Only, 63.5mm O.D. x 117mm Length, Bushing Size/15
150mL Heavy Wall Pressure Vessel, Round Bottom, #15 Internal Thread, Vessel Only, 63.5mm O.D. x 117mm Length, Bushing Size/15. Heavy wall pressure vessels have an internal thread for use with PTFE bushings as pressure seals. The design allows hand tightening/loosening for easy access into the vessel. O-ring is positioned on the bushing above the thread for improved sealing. Supplied complete with vessel, PTFE bushing & Viton o-ring. Optional Perfluoro o-ring has the chemical resistance & service temperature range similar to Kalrez 4079. See CG-362, CG-364, and CG-366 for optional PTFE Bushings.IMPORTANT NOTICE: ALL CHEMGLASS PRESSURE VESSELS ARE TESTED AT 150 PSI, OR APPROX TWO AND ONE-HALF TIMES THEIR RECOMMENDED WORKING PRESSURE. HOWEVER, CHEMGLASS DOES NOT GUARANTEE THE VESSEL FROM BREAKING UNDER PRESSURE, DUE TO THE NATURE OF MATERIAL AND CONDITIONS BEYOND OUR CONTROL. CHEMGLASS RECOMMENDS THE USE OF SAFETY SHIELDS AND/OR OTHER SAFETY EQUIPMENT.
Hach Company GAS BUBBLER, MDM DIFFUSION TUBE
Designed for use with the General Purpose Distillation Apparatus. Round bottom, 500 mL capacity. Long neck with branch and thermometer port. Neck extends 90 mm above flask body and branch extends 150 mm above flask body. Both neck and branch have 20-400 screw-thread finish. Thermometer port has 13-425 screw-thread finish.
Hach Company Condenser
Designed for use with the General Purpose Distillation Apparatus. Round bottom, 500 mL capacity. Long neck with branch and thermometer port. Neck extends 90 mm above flask body and branch extends 150 mm above flask body. Both neck and branch have 20-400 screw-thread finish. Thermometer port has 13-425 screw-thread finish.
Hach Company CYLINDER, SINGLE LINE 24-400
Replacement cylinder for distillation apparatus set 2265300.
Chemglass Life Sciences J-Kem Temperature Controller, Model 260/T, Type "J" (-0°C to 800°C), Complete
J-Kem Temperature Controller, Model 260/T, Type "J" (-0C to 800C), Complete. The Model 260/T disconnects all output power it the process temperature exceeds the entered temperature by a user-specified amount, or following recovery from a power failure. The outputs remain disconnected until manually reset. Over temperature condition is signalled by an indicator lamp and audible alarm. The Model 260/T has 1800 Watts of power which is sufficient for heating mantles up to 22L. Controller has the ability to display temperature without heating. The Model 260/T is also equipped with a100 hour digital timer to turn heating ON or OFF when time has expired.PLEASE NOTE: THE TYPE T, J AND K CONTROLLERS ARE SUPPLIED COMPLETE WITH: 1/8 DIAMETER X 12 LONG PTFE COATED THERMOCOUPLE, 10FT COILED EXTENSION CORD, AND A 14/20 PTFE THERMOCOUPLE ADAPTER. Specifications:Dimensions: 3.25" H x 7.5" W x 9" DPower: 15 Amps @ 120VAC, 1800 Watts
Chemglass Life Sciences Distilling Head, Short Path, Jacketed, 10/18 Thermometer Joint, 14/20 Lower Inner Joint, Approx. 105mm Width x 105mm Height
Distilling Head, Short Path, Jacketed, 10/18 Thermometer Joint, 14/20 Lower Inner Joint, Approx. 105mm Width x 105mm Height. Similar to CG-1239 but vacuum jacketed to improve efficiency. Available with Vigreux indentations in uptake tube to further increase the performance of the head. NOTE: The 14/20 size accepts a 1” immersion 7/12 or 10/18 thermometer, while the 24/40 and 29/42 sizes accept a 2” immersion, 10/30 thermometer.
Chemglass Life Sciences Distilling Head, Short Path, Vigreux Indents, 10/30 Thermometer Joint, 24/40 Lower Inner Joint, Approx. 195mm Width x 160mm Height
Distilling Head, Short Path, Vigreux Indents, 10/30 Thermometer Joint, 24/40 Lower Inner Joint, Approx. 195mm Width x 160mm Height. Designed for use with small quantities where hold up between the flask and receiver must be kept to a minimum. The thermometer bulb and stem serve as column packing. Upper hose connections are for cooling lines while the lower connection is for vacuum. Available with Vigreux indentations to improve efficiency. NOTE: The 14/20 size accepts a 1” immersion 7/12 or 10/18 thermometer, while the 24/40 and 29/42 sizes accepts a 2” immersion, 10/30 thermometer.
Chemglass Life Sciences Condenser, Reflux, 565mm, 24/40 Joint, Style B, 400mm Jacket Length
Condenser, Reflux, 565mm, 24/40 Joint, Style B, 400mm Jacket Length. Coil style reflux condenser with tightly wrapped coil providing maximum cooling. Excellent for use with high vapor pressure solvents. Condenser has a top outer standard taper joint and lower inner drip tip joint. Hose connections have an O.D. of 10mm at the middle serration.